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Phthalonitrile-based High Temperature Resin

T. Keller
Published 1988 · Chemistry

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An aromatic, diether-linked phthalonitrile resin, prepared from 4,4′-bis(3,4-dicyanophenoxy)biphenyl, exhibits excellent thermo-oxidative properties. The resin is easily processed from the melt of the monomer in a controlled manner as a function of the amine curing agent and processing temperatures. Polymerization occurs by a cyclic addition reaction without the formation of volatile by-products. The polymerization reaction can be stopped at a prepolymer stage. The prepolymer can be stored indefinitely at ambient conditions without further reaction. The modulus and viscoelastic properties of the resin were found to be a function of the postcuring conditions.



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