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Synthesis Of N-doped SWNT Using The Arc-discharge Procedure

M. Glerup, M. Glerup, J. Steinmetz, J. Steinmetz, D. Samaille, O. Stéphan, S. Enouz, Annick Loiseau, S. Roth, P. Bernier
Published 2004 · Materials Science

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Single-walled nitrogen doped nanotubes were prepared using two novel approaches in an arc-discharge process. In both cases a nitrogen-rich precursor was introduced into the anode rods together with graphite and the catalysts. The nitrogen rich precursors were organic and inorganic, respectively. Both synthesis routes gave nanotubes with a nitrogen concentration of a maximum of 1%, determined using electron energy loss spectroscopy (EELS) coupled with transmission electron microscopy (TEM). All samples were characterized with scanning electron microscopy (SEM), TEM, and high-resolution transmission electron microscopy (HRTEM).
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