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Use Of Isothermal Titration Calorimetry To Study Surfactant Aggregation In Colloidal Systems.

W. Loh, César Brinatti, K. C. Tam
Published 2016 · Chemistry, Medicine

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BACKGROUND Isothermal titration calorimetry (ITC) is a general technique that allows for precise and highly sensitive measurements. These measurements may provide a complete and accurate thermodynamic description of association processes in complex systems such as colloidal mixtures. SCOPE OF THE REVIEW This review will address uses of ITC for studies of surfactant aggregation to form micelles, with emphasis on the thermodynamic studies of homologous surfactant series. We will also review studies on surfactant association with polymers of different molecular characteristics and with colloidal particles. GENERAL SIGNIFICANCE ITC studies on the association of different homologous series of surfactants provide quantitative information on independent contribution from their apolar hydrocarbon chains and polar headgroups to the different thermodynamic functions associated with micellization (Gibbs energy, enthalpy and entropy). Studies on surfactant association to polymers by ITC provide a comprehensive description of the association process, including examples in which particular features revealed by ITC were elucidated by using ancillary techniques such as light or X-ray scattering measurements. Examples of uses of ITC to follow surfactant association to biomolecules such as proteins or DNA, or nanoparticles are also highlighted. Finally, recent theoretical models that were proposed to analyze ITC data in terms of binding/association processes are discussed. MAJOR CONCLUSIONS This review stresses the importance of using direct calorimetric measurements to obtain and report accurate thermodynamic data, even in complex systems. These data, whenever possible, should be confirmed and associated with other ancillary techniques that allow elucidation of the nature of the transformations detected by calorimetric results, providing a complete description of the process under scrutiny.
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Isothermal titration calorimetry and surface plasmon resonance analysis using the dynamic approach
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Development of food-grade Pickering oil-in-water emulsions: Tailoring functionality using mixtures of cellulose nanocrystals and lauric arginate.
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Isothermal Titration Calorimetry: Principles and Applications
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Thermal Activity in Affinity Separation Techniques Such as Liquid–Liquid Extraction Analyzed by Isothermal Titration Calorimetry and Accuracy Analysis of the Technique in the Molar Concentration Domain
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Studies on the self-aggregation, interfacial and thermodynamic properties of a surface active imidazolium-based ionic liquid in aqueous solution: Effects of salt and temperature
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Cationic gemini surfactant as a dual linker for a cholic acid-modified polysaccharide in aqueous solution: thermodynamics of interaction and phase behavior.
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Intermolecular Interactions in Polyelectrolyte and Surfactant Complexes in Solution
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Can the Isothermal Calorimetric Curve Shapes Suggest the Structural Changes in Micellar Aggregates?
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Development of nanofibrous membranes for enzymatic food processing
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