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Optimization Of Gas Chromatographic Method For The Enantioseparation Of Arylpropionic Non-steroidal Anti-inflammatory Drug Methyl Esters.

Marinko Petrović, Zeljko Debeljak, Nikola Blažević
Published 2005 · Chemistry, Medicine
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The gas chromatography (GC) method for enantioseparation of well-known non-steroidal anti-inflammatory drugs ibuprofen, fenoprofen and ketoprofen methyl esters mixture was developed. Best enantioseparation was performed on capillary column with heptakis-(2,3-di-O-methyl-6-O-t-butyldimethyl-silyl)-beta-cyclodextrin stationary phase and hydrogen used as a carrier gas. Initial temperature, program rate and carrier pressure were optimized to obtain best resolution between enantiomers.



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