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Colorimetric And Ratiometric Sensors Derivated From Natural Building Blocks For Fluoride Ion Detection

Heng Shi, Fengfei Zhao, Xinghan Chen, Shilong Yang, Jieni Xing, H. Chen, R. Zhang, J. Liu
Published 2019 · Chemistry

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Abstract Three novel colorimetric and ratiometric probes (SH-1~3) for fluoride ion detection were designed and synthesized from nature small molecules. Obvious yellow-to-orange color change of these probes in the THF was achieved only in presence of F− among the eight anions (F−, Cl−, Br−, I−, H2PO4−, HSO4−, CH3COO–, ClO4−), along with the emission shifting from green to orange red. These three probes are 1:1 complexed with fluoride ions, with complexation constant of around 0.1 × 104 M−1. The detection limit of probes SH-1~3 reached as low as around 1 μM. 1H NMR titration study suggested that the fluoride ion induced deprotonation of the probe through hydrogen bonding interaction between amino group of probe and fluoride ion.
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