Online citations, reference lists, and bibliographies.
← Back to Search

Size-Controlled Synthesis Of Iron And Iron Oxide Nanoparticles By The Rapid Inductive Heating Method

Pratikshya Sharma, Noah Holliger, P. Pfromm, B. Liu, Viktor Chikan
Published 2020 · Materials Science, Medicine

Cite This
Download PDF
Analyze on Scholarcy
Share
Inductive heating synthesis is an emerging technique with the potential to displace the hot-injection synthesis method to prepare colloidal particles very rapidly with a narrow size distribution, controlled size, and high crystallinity. In this work, the inductive heating synthesis is applied to produce a short-temperature jump to mimic conditions like the hot-injection method to prepare traditional iron and iron oxide nanoparticles (IONPs) in the 3–11 nm size range within various solvents, precursors, and reaction time conditions. Moreover, this inductive heating technique can be used under unique experimental conditions not available for hot-injection reactions. These conditions include the use of very high initial monomer concentrations. Considering benefits over conventional methods, the inductive heating technique has the potential to provide an industrial level scale-up synthesis. The magnetization of these particles is consistent with the magnetization of the particles from the literature.
This paper references
10.1002/ANIE.200602866
Magnetic nanoparticles: synthesis, protection, functionalization, and application.
A. Lu (2007)
10.1021/CG060656P
Synthesis of Amine-stabilized Aqueous Colloidal Iron Oxide Nanoparticles.
M. Aslam (2007)
10.1021/JA00072A025
Synthesis and characterization of nearly monodisperse CdE (E = sulfur, selenium, tellurium) semiconductor nanocrystallites
C. Murray (1993)
Synthesis of Highly Crystalline and Monodisperse Maghemite Nanocrystallites ACS Omega
T Hyeon
Appearance of Superparamagnetism on Heating Nanosize Mn 0 . 65 Zn 0 . 35 Fe 2 O 4
C. Rath (2000)
10.1021/IE070494+
Processing of Iron Oxide Nanoparticles by Supercritical Fluids
U. T. Lam (2008)
10.1016/0304-8853(95)00365-7
Advances in ferrofluid technology
K. Raj (1995)
10.1016/J.APSUSC.2014.09.181
Magnetic properties of novel superparamagnetic iron oxide nanoclusters and their peculiarity under annealing treatment
M. Tadić (2014)
10.1016/J.MATCHAR.2018.12.014
Synthesis, particle shape characterization, magnetic properties and surface modification of superparamagnetic iron oxide nanochains
Marin Tadic (2019)
10.1021/JA026501X
Size-controlled synthesis of magnetite nanoparticles.
S. Sun (2002)
10.1016/J.PCRYSGROW.2008.08.003
Synthesis, properties, and applications of magnetic iron oxide nanoparticles
A. Teja (2009)
10.1007/s11671-008-9174-9
Magnetic Iron Oxide Nanoparticles: Synthesis and Surface Functionalization Strategies
W. Wu (2008)
10.1021/cr068445e
Magnetic iron oxide nanoparticles: synthesis, stabilization, vectorization, physicochemical characterizations, and biological applications.
S. Laurent (2008)
10.1016/J.COLSURFA.2006.04.027
Synthesis of monodisperse maghemite nanoparticles by the microemulsion method
J. Vidal-Vidal (2006)
10.1021/acsomega.8b00096
Rapid Induction and Microwave Heat-Up Syntheses of CdSe Quantum Dots
Hongfu Luo (2018)
10.1016/J.BIOMATERIALS.2004.10.012
Synthesis and surface engineering of iron oxide nanoparticles for biomedical applications.
A. Gupta (2005)
Size-Selection Process
(2001)
10.1088/1468-6996/16/2/023501
Recent progress on magnetic iron oxide nanoparticles: synthesis, surface functional strategies and biomedical applications
Wei Wu (2015)
10.1021/JA034813+
Structural tuning of charge, orbital, and spin ordering in double-cell perovskite series between NdBaFe(2)O(5) and HoBaFe(2)O(5).
P. Woodward (2003)
10.2147/NSA.S99986
Synthesis, characterization, applications, and challenges of iron oxide nanoparticles
Attarad Ali (2016)
10.1007/BF00202677
The infrared dielectric properties of maghemite, γ-Fe2O3, from reflectance measurement on pressed powders
C. Pecharromán (1995)
10.1088/0953-8984/22/25/255401
Vacancy ordering and electronic structure of γ-Fe₂O₃ (maghemite): a theoretical investigation.
Ricardo Grau-Crespo (2010)
10.1016/S0079-6816(01)00056-9
Surface chemistry and catalysis on well-defined epitaxial iron-oxide layers
W. Weiss (2002)
10.1016/J.JALLCOM.2019.03.414
Hydrothermal synthesis of hematite (α-Fe2O3) nanoparticle forms: Synthesis conditions, structure, particle shape analysis, cytotoxicity and magnetic properties
Marin Tadic (2019)
A Powder Neutron Diffraction Investigation of Vacancy Ordering and Covalence in γ - Fe 2 O 3
C. Greaves (1983)
10.1021/acsnano.7b00609
Thermal Decomposition Synthesis of Iron Oxide Nanoparticles with Diminished Magnetic Dead Layer by Controlled Addition of Oxygen.
M. Unni (2017)
10.1021/CM302229B
Facile Synthesis of Germanium Nanoparticles with Size Control: Microwave versus Conventional Heating
Elayaraja Muthuswamy (2013)
Crystal Structure and Isothermal Compression of Fe 2 O 3 , Cr 2 O 3 , and V 2 O 3 to 50 Kbars
L. W. Finger (1980)
10.1063/1.1728716
Exchange Anisotropy—A Review
W. Meiklejohn (1962)
10.2478/jee-2019-0044
Magnetic properties of hematite (α − Fe2O3) nanoparticles synthesized by sol-gel synthesis method: The influence of particle size and particle size distribution
M. Tadić (2019)
10.1021/JA016812S
Synthesis of highly crystalline and monodisperse maghemite nanocrystallites without a size-selection process.
T. Hyeon (2001)
10.1039/C6RA05064F
Core/shell iron/iron oxide nanoparticles: are they promising for magnetic hyperthermia?
Z. Nemati (2016)
10.1021/JA063969H
Synthesis and stabilization of monodisperse Fe nanoparticles.
S. Peng (2006)
10.1016/J.APSUSC.2019.01.098
Iron oxide nanochains coated with silica: Synthesis, surface effects and magnetic properties
M. Tadić (2019)
10.1039/B207789B
Chemical synthesis of magnetic nanoparticles.
T. Hyeon (2003)
10.3390/nano6050085
Rapid Nanoparticle Synthesis by Magnetic and Microwave Heating
Viktor Chikan (2016)
10.1109/20.809134
Thermal effect limits in ultrahigh-density magnetic recording
D. Weller (1999)
10.1039/c8nr03026j
The influence of polyethylene glycol passivation on the surface plasmon resonance induced photothermal properties of gold nanorods.
R. Marasini (2018)
10.1038/NMAT1251
Ultra-large-scale syntheses of monodisperse nanocrystals
J. Park (2004)
10.1039/C3TB00369H
Scaling Laws at the Nano Size: The Effect of Particle Size and Shape on the Magnetism and Relaxivity of Iron Oxide Nanoparticle Contrast Agents.
Eric D. Smolensky (2013)
10.1088/0957-4484/24/17/175601
Alternative low-cost approach to the synthesis of magnetic iron oxide nanoparticles by thermal decomposition of organic precursors.
I. O. Perez De Berti (2013)
10.1016/S0304-8853(98)00845-2
Anomalous properties of magnetic nanoparticles
A. Berkowitz (1999)



Semantic Scholar Logo Some data provided by SemanticScholar