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(E)-α,β-unsaturated Amides From Tertiary Amines, Olefins And CO Via Pd/Cu-catalyzed Aerobic Oxidative N-dealkylation

Renyi Shi, Hua Zhang, Lijun Lu, Pei Gan, Yuchen Sha, Heng Zhang, Qiang Liu, Matthias Beller, Aiwen Lei

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A novel Pd/Cu-catalyzed chemoselective aerobic oxidative N-dealkylation/carbonylation reaction has been developed for the efficient and straightforward construction of synthetically useful and bioactive (E)-α,β-unsaturated amide derivatives.