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Synthesis Of Thioureido-linked Peptidomimetics, Glycosylated Amino Acids, And Neoglycoconjugates Using Bis(benzotriazolyl)methanethione As Thioacylating Agent
Published 2010 · Chemistry
A practical synthesis of thiourea-linked peptidomimetics, glycosylated amino acids, and neoglycoconjugates is described employing bis(benzotriazolyl) methanethione as thiocarbonylating reagent. The entire protocol is mild, efficient, high-yielding, and free from hazardous reagents. All the intermediates and products have been isolated and fully characterized by 1H NMR, 13C NMR, and mass spectrometry. Â© Georg Thieme Verlag Stuttgart â¢ New York.