Online citations, reference lists, and bibliographies.
← Back to Search

3-(4-Chloroanilino)-5,5-dimethylcyclohex-2-en-1-one

S. Anthal, A. Sambyal, R. Bamzai, R. Kant, V. Gupta
Published 2012 · Chemistry, Medicine, Computer Science

Cite This
Download PDF
Analyze on Scholarcy
Share
The asymmetric unit of the title compound, C14H16ClNO, contains two independent molecules, both with the cyclohexene ring in a sofa conformation. In the crystal, N—H⋯O hydrogen bonds link the molecules related by translation along the a axis into two crystallographically independent chains. Weak C—H⋯π interactions are also observed.
This paper references
) C2B-C3B-N1B-C9B 2.0 (4) C2A-C1A-C6A-C5A −34.1 (3) C4B-C3B-N1B-C9B −176
10.1021/JO01086A010
Synthesis of Tetrahydrocarbazoles and Carbazoles by the Bischler Reaction1,2
E. Campaigne (1959)
10.1107/S0108768197008677
Intermolecular N-H...O hydrogen bonding assisted by resonance. II. Self assembly of hydrogen-bonded secondary enaminones in supramolecular catemers
V. Bertolasi (1998)
10.1107/S090744490804362X
Structure validation in chemical crystallography
A. Spek (2009)
) C3B-C4B-C5B-C7B 171.04 (19) C13A-C14A-C9A-N1A −178.7 (2) C3B-C4B-C5B-C8B −68.2 (3) C11A-C10A-C9A-C14A −1.8 (3) C3B-C4B-C5B-C6B
C1A-C6A-C5A-C8A 174.3 (2) Cl1B-C12B-C13B-C14B 178
CrysAlis PRO and CrysAlis RED
(2010)
10.1039/P298700000S1
Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds
F. Allen (1987)
10.1021/JO00056A006
Additions of 1-(aminomethyl)benzotriazoles to enamines, enamides, and vinyl ethers: novel routes to 1,3-diamines and tetrahydroquinolines
A. R. Katritzky (1993)
10.1021/OL060570P
1,3-diketones from acid chlorides and ketones: a rapid and general one-pot synthesis of pyrazoles.
S. T. Heller (2006)
Special details Experimental. CrysAlis PRO, Oxford Diffraction Ltd., Version 1.171.34.40 (release 27–08-2010 CrysAlis171
Flack (2010)
10.1107/S1600536810033933
3-(2-Amino-5-nitroanilino)-5,5-dimethylcyclohex-2-en-1-one 0.25-hydrate
S. Mehdi (2010)
C3A-C4A-C5A-C8A −170.3 (2) C3B-N1B-C9B-C14B 122.7 (2) C3A-C4A-C5A-C7A 69.3 (2) C3B-N1B-C9B-C10B −58
10.1107/S0021889897003117
ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI)
L. Farrugia (1997)
10.1107/S0108767383001762
On enantiomorph‐polarity estimation
H. Flack (1983)
o2414–o2415. Oxford Diffraction
E Cryst. (2010)
10.1107/S0108767307043930
A short history of SHELX.
G. Sheldrick (2008)
10.1515/9783111576855-015
J
Seguin Hen (1824)
C6A-C1A-C2A-C3A 6.0 (3) C2B-C1B-C6B-C5B
Acta Cryst
Diffraction Ltd (2008)



Semantic Scholar Logo Some data provided by SemanticScholar