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Caracterización De Suspensiones Coloidales De Nanopartículas Metálicas Sintetizadas Por Ablación Láser De Pulsos Ultracortos

D. M. Arboleda
Published 2018 · Materials Science

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xii composition of the colloids, the technique of optical extinction spectroscopy (OES) is mainly used, and for its complementation, techniques are independently used such as Atomic force microscopy, (AFM), transmission electron microscopy (TEM), electron diffraction (ED), Raman and microRaman spectroscopy, scattering of X-rays at small angle (SAXS), z potential and, for some colloids, their magnetic response is analyzed by means of vibrating sample magnetometry (VSM). Particularly in the case of Ag, in addition to the morphological characterization, structure and size, the analysis of long-term stability of the colloidal suspensions is carried out, using stabilizing agents such as soluble starch (st) and trisodium citrate (TSC). The theoretical aspect of this Thesis covers a qualitative and quantitative description of the dielectric function of metals at the nanoscale, analyzing the dependence with size for radii less than 10 nm, and the development of a novel linear regression method for the determination of the values of the plasma frequency ωp and the damping constant γlibre, from the adjustment of the bulk experimental dielectric function for low frequencies (long wavelengths) using the Drude model. These parameters are determined for metals such as Au, Ag, Cu, Ni, Mo, W, Pb, Zn and Na, with which it is possible to model the size-dependent dielectric function. With the development of this modeling and Mie theory, the experimental extinction spectra of Ag and Ni (OES technique) are theoretically analyzed and fitted, reproducing computationally the optical response of their colloids, to later determine the composition, structure and sizes distribution of the NPs synthesized. On the other hand, the presence of metal clusters of few atoms in the colloidal suspensions formed during the synthesis by laser ablation of femtoseconds in solution (FLASiS), is analyzed by means of their fluorescence. This analysis is developed based on the energy used for the synthesis, providing the possibility of determining the fluence of the laser that generates clusters with higher luminescence. The formation of fractals
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