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Radical Carbonylations Using A Continuous Microflow System

Takahide Fukuyama, Md Taifur Rahman, Naoya Kamata, Ilhyong Ryu

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Radical-based carbonylation reactions of alkyl halides were conducted in a microflow reactor under pressurized carbon monoxide gas. Good to excellent yields of carbonylated products were obtained via radical formylation, carbonylative cyclization and three-component coupling reactions, using tributyltin hydride or TTMSS as a radical mediator.