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Methyl Ketones From Carboxylic Acids: Cyclohexyl Methyl Ketone
Published 2003 · Chemistry
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Methyl ketones from carboxylic acids: cyclohexyl methyl ketone solvent: Commercial 1,2-dimethoxyethane, b.p. 85–86°, purchased from Eastman Organic Chemicals, was distilled from lithium aluminum hydride before use reactant: cyclohexanecarboxylic acid, m.p. 31–32°, purchased from Aldrich Chemical Company was used without further purification product: cyclohexyl methyl ketone Keywords: addition, to CO; Grignard and related reactions; assay methods, for methyllithium with 2-butanol, 1,10-phenanthroline or 2,2'-bipydridyl or 2,2'-biquinoline indicator; 1,2-dimethoxyethane, purification of; hydrogen, fire hazard