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Rapid Identification And Estimation Of Gitoxin In Digitoxin And Digoxin Tablets By TLC.

M. L. Dow, R. D. Kirchhoefer, J. Brower
Published 1971 · Chemistry, Medicine

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A rapid TLC procedure was developed for the identification and estimation of gitoxin in digitoxin and digoxin tablets. A solution of tablet material is spotted on a TLC plate directly, and the gitoxin is estimated by visual comparison of fluorescence with that of standards after spraying with acid-ferric chloride T.S. USP XVII. The method can detect 0.5% of gitoxin in the presence of 1 mcg. of cardiac glycosides.
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