Online citations, reference lists, and bibliographies.
← Back to Search

Separation Of Solanesol In Tobacco Leaves Extract By Slow Rotary Counter-current Chromatography Using A Novel Non-aqueous Two-phase Solvent System.

Yang Zhao, Q. Du
Published 2007 · Chemistry, Medicine

Save to my Library
Download PDF
Analyze on Scholarcy
Share
Non-aqueous solvent system composed of sunflower oil-ethanol was found to be suitable for the separation of lower polarity components. Employing this solvent system, 3 g of tobacco leaves extract containing 15% solanesol was separated using a slow rotary counter-current chromatograph equipped with an 1100 mL column made of 5.7 mm I.D. convoluted PTFE tube. The separation yielded 1.5 g of yellow oily product in which solanesol occupied 26.8% determined by HPLC. The tobacco tar and other main impurities in the tobacco leaves extract were removed after slow rotary counter-current chromatographic separation. The separation processing may be developed as a technique for producing a solanesol product with food grade.
This paper references



This paper is referenced by
10.1007/s11101-014-9348-2
Counter-current chromatography for the separation of terpenoids: a comprehensive review with respect to the solvent systems employed
K. Skalicka-Woźniak (2014)
10.1080/01496390903566713
Enrichment and Purification of Total Chlorogenic Acids from Tobacco Waste Extract with Macroporous Resins
Zhao Hui (2010)
10.1002/jssc.201501199
Developments in high-speed countercurrent chromatography and its applications in the separation of terpenoids and saponins.
H. Song (2016)
10.1080/15685551.2015.1070495
Preparation and adsorption property of solanesol molecular imprinted polymers
Jiapeng Long (2015)
10.3724/SP.J.1009.2008.00013
Methodology Research of High-speed Counter-current Chromatography in Separation of Natural Products: Methodology Research of High-speed Counter-current Chromatography in Separation of Natural Products
Shun Yao (2009)
10.1080/10826076.2016.1230552
Selection of a nonaqueous two-phase solvent system for fractionation of xylo-oligosaccharide prebiotics using a conductor-like screening model for real solvents
H. Zhang (2016)
10.1016/J.SEPPUR.2015.03.016
Simultaneous extraction of nicotine and solanesol from waste tobacco materials by the column chromatographic extraction method and their separation and purification
R. Hu (2015)
10.1016/J.JPBA.2007.10.014
Continuous counter current extraction, isolation and determination of solanesol in Nicotiana tobacum L. by non-aqueous reversed phase high performance liquid chromatography.
R. N. Rao (2008)
10.1007/BF03160818
Literature cited
L. Stockwell (2009)
10.1016/j.talanta.2010.06.037
Fast determination of chlorogenic acid in tobacco residues using microwave-assisted extraction and capillary zone electrophoresis technique.
Z. Li (2010)
10.1016/j.chroma.2017.01.058
Enhancing silymarin fractionation using the conductor-like screening model for real solvents.
Emma C. Brace (2017)
10.3390/biom9080334
Bioactivities and Medicinal Value of Solanesol and Its Accumulation, Extraction Technology, and Determination Methods
Ning Yan (2019)
10.1007/978-1-61779-624-1_9
Separation of natural products by countercurrent chromatography.
J. McAlpine (2012)
10.1557/JMR.2019.148
Noble surface molecularly imprinted polymer modified titanium dioxide toward solanesol adsorption selectivity study
Chenglong Duan (2019)
10.1016/J.BEJ.2008.06.002
Bioactivity of solanesol extracted from tobacco leaves with carbon dioxide–ethanol fluids
Wen Huang (2008)
10.1109/ICMREE.2013.6893826
A new method of extraction and purification of solanesol from tobacco extracts
Zhenggui Gu (2013)
Extraction, Isolation and Purification of Solanesol obtained from Nicotiana tobaccum
N. D. Thombare (2015)
A NEW METHOD OF EXTRACTION, ISOLATION AND DETERMINATION OF SOLANESOL FROM TOBACCO WASTE (NICOTIANA TOBACUM L.) BY NON-AQUEOUS RP-HPLC
Srinivasa Rao Atla (2014)
10.1016/j.chroma.2010.07.037
A novel method for analyzing solanesyl esters in tobacco leaves using atmospheric pressure chemical ionization/mass spectrometer.
N. Ishida (2010)
Feasibility of Extracting Solanesol from Tobacco Biomass as a Byproduct Following Protein Recovery
P. Machado (2008)
10.1016/j.phytochem.2011.03.015
Solanesol: added value from Solanaceous waste.
M. Taylor (2011)
10.1016/j.chroma.2011.06.082
Expanded separation technique for chlorophyll metabolites in Oriental tobacco leaf using non aqueous reversed phase chromatography.
N. Ishida (2011)
10.5897/AJB2009.000-9220
Application of response surface methodology optimization for the production of caffeic acid from tobacco waste
J. Wang (2009)
S0884291419001481 3271..3287
Chenglong Duan (2019)
Enhancing Silymarin Fractionation via Molecular Modeling using the Conductor-like Screening Model for Real Solvents
Emma C. Brace (2016)
Semantic Scholar Logo Some data provided by SemanticScholar