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CuSCN-Mediated Homocoupling Of Terminal Alkynes To 1,3-Diynes Using 4-Nitrobenzenediazonium Tetrafluoroborate As Oxidant

Haidong Liu, Bo Chen, Jin Cai, Junqing Chen, Min Ji

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Eleven 1,3-diynes have been prepared by a highly efficient base-catalysed homocoupling of terminal alkynes mediated by a novel combination of CuSCN/4-nitrobenzenediazonium tetrafluoroborate.